This research is studied about using small scale titration kit for teaching lab titration in analytical chemistry for 4th years of teacher-student. This research aimed 1) to examine effective of the small-scale titration kit, 2) to compare pre-test and post-test scores of students through using small scale set titration and 3) to study the students' satisfaction towards learning by using developed small scale titration kit. The results showed that the efficiency of learning kit was 76.83/78.44 which reached the standard as 75/75 criterions, the analysis of pre-test and post-test scores was examined using the paired-samples t-test analysis, the means score collected from the post-achievement test was 12.20 which was significantly higher than those collected from the pre-achievement test, 9.70, (p<0.05) and students’ satisfaction in learning was in the high level. Moreover, the small-scale titration kit requires a small amount of reagent, used a low-cost material. It is easy for teachers to develop from local materials for using in their classroom.